Another vote for Ornstien and Smough. Died a couple of times, first time I had an NPC phantom fighting Smough which let me solo Ornstien. I wasn't ready for 'lightning Smough' after that, though. Second time, I killed Smough first and my phantom died so I had to solo beefy Ornstein. Third time, I won without getting hit (of course).
IMO, lightning Smough is much easier than huge Ornstein, as he doesn't quite have the speed and he is weak to fire.
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